University of Oxford
Mass Spectrometry Research Facility
Chemistry Research Laboratory, University of Oxford
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Service LC-MS (Exactive)

Image of a Thermo Exactive mass spectrometer

MS Staff Member:
Victor Mikhailov

Location:
Basement MS Annex (00.086A)

Booking:
N/A

Training required:
N/A, only by special arrangement for specific projects or collaborations

Instrument description:

Thermo Exactive High-Resolution Orbitrap FTMS normally used for MS services without front end LC in direct infusion (loop injection) mode. Currently connected to an Acquity Column Manager, Acquity Sample Manager, Acquity Binary Solvent Manager and Acquity TUV Detector.

Typical applications:

Fast mass analysis of purified samples up to 4000 m/z, LC-MS analysis

Agilent GC-MSD User Information

Alternative Ionisation

Bruker MALDI Sample Preparation

Combining Trypsin/Chymotrypsin Enzymatic Digestion

ESI Accurate Mass

External Services

GC-MS (Agilent 7200)

In-Gel Trypsin Enzymatic Digestion

In-solution Chymotrypsin Enzymatic Digestion

In-solution protein digestion

MALDI Oligonucleotide Sample Preparation

MALDI User Information

Native MS Sample Preparation

Preparation of blood plasma for metabolomics

Preparation of cell samples for metabolomics

Preparation of plant samples for metabolomics

Preparation of tissue samples for metabolomics

Proteomics Service

Rapid Digestion - Promega Trypsin/Lys-C Kit

RP-HPLC Purification of Oligonucleotides

Sample Preparation Protocol for Alternative Ionisation Service

Sample Preparation Protocol for BioAccord 1 Intact Protein Analysis

Sample Preparation Protocol for BioAccords

Sample Preparation Protocol for ESI Accurate Mass Service

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